Sắc Ký Đồ Các Mẫu Thẩm Định Độ Lặp Lại

3/21/2019 7:04:46 PM Page 1 / 1

Analysis Report

Sample Name :

Sample ID :

Data Filename : oxo chuan 6.25ug 19-3-2019.lcd

Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/19/2019 8:15:58 PM Acquired by : System Administrator Date Processed : 3/19/2019 8:36:43 PM Processed by : System Administrator

mAU

PDA Multi 1 254nm,4nm

14.165

12.5

10.0

7.5

5.0

2.595

2.5

2.243

2.475

0.0

0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0

min

PDA Ch1 254nm

Peak#

Ret. Time	Area	Height	Conc.	Unit	Mark	Name
1	2.243	3210	348	0.000
2	2.475	3077	408	0.000		V
3	2.595	23768	2617	0.000		V
4	14.165	418469	11975	0.000
Total		448525	15348

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D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 6.25ug 19-3-2019.lcd

5/3/2019 12:34:40 PM Page 1 / 1

Analysis Report

Sample Name :

Sample ID :

Data Filename : oxo chuan 12.5ug 19-3-2019.lcd

Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/19/2019 7:53:40 PM Acquired by : System Administrator Date Processed : 3/19/2019 8:14:25 PM Processed by : System Administrator

mAU

PDA Multi 1 254nm,4nm

14.131

2.589

0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0

min

PDA Ch1 254nm

Peak#

Ret. Time	Area	Height	Conc.	Unit	Mark	Name
1	2.589	20242	2277	0.000
2	14.131	696245	20198	0.000
Total		716486	22475

D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 12.5ug 19-3-2019.lcd

5/3/2019 12:34:37 PM Page 1 / 1

Analysis Report

Sample Name :

Sample ID :

Data Filename : oxo chuan 25ug 19-3-2019.lcd

Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/19/2019 7:30:36 PM Acquired by : System Administrator Date Processed : 3/19/2019 7:51:39 PM Processed by : System Administrator

14.111

mAU

PDA Multi 1 254nm,4nm

2.589

3.288

0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0

min

PDA Ch1 254nm

Peak#

Ret. Time	Area	Height	Conc.	Unit	Mark	Name
1	2.589	18451	2032	0.000
2	3.288	5923	131	0.000
3	14.111	1214153	34814	0.000
Total		1238527	36978

D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 25ug 19-3-2019.lcd

5/3/2019 12:34:32 PM Page 1 / 1

Analysis Report

Sample Name :

Sample ID :

Data Filename : oxo chuan 50ug 19-3-2019.lcd

Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/19/2019 7:01:24 PM Acquired by : System Administrator Date Processed : 3/19/2019 7:22:26 PM Processed by : System Administrator

mAU

PDA Multi 1 254nm,4nm

14.069

2.591

3.288

0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0

min

PDA Ch1 254nm

Peak#

Ret. Time	Area	Height	Conc.	Unit	Mark	Name
1	2.591	13294	1671	0.000
2	3.288	6211	181	0.000
3	14.069	2506725	71991	0.000
Total		2526229	73842

D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 50ug 19-3-2019.lcd

5/3/2019 12:34:40 PM Page 1 / 1

Analysis Report

Sample Name :

Sample ID :

Data Filename : oxo chuan 100ug 19-3-2019.lcd

Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/19/2019 6:35:20 PM Acquired by : System Administrator Date Processed : 3/19/2019 6:56:22 PM Processed by : System Administrator

mAU

PDA Multi 1 254nm,4nm

13.725

125

100

2.204 2.571

2.675 3.019

3.236

0.324

0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0

min

PDA Ch1 254nm

Peak#

Ret. Time	Area	Height	Conc.	Unit	Mark	Name
1	0.324	37725	7640	0.000
2	2.204	1005	151	0.000
3	2.571	4291	1236	0.000
4	2.675	12020	1079	0.000		V
5	3.019	2780	232	0.000
6	3.236	1322	181	0.000		V
7	13.725	4900220	135794	0.000
Total		4959363	146313

D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 100ug 19-3-2019.lcd

Phụ lục 4.3.3. Sắc ký đồ các mẫu thẩm định độ lặp lại

3/21/2019 7:04:14 PM Page 1 / 2

Analysis Report

Sample Name : Mau chiet 1 Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH-1-20-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename : oxo-batch-20-03-2019.lcb

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/20/2019 8:19:47 PM Acquired by : System Administrator Date Processed : 3/21/2019 10:33:23 AM Processed by : System Administrator

mAU

PDA Multi 1 254nm,4nm

5.348

13.981

25.818

262.155.5537

26.474

33.615

24.705

26.921

27.154

2.385

2.566

2.942

3.307

3.534

4.414

6.783

7.168

6.261

12.459

25.134

27.734

28.020

28.395

30.059

31.474

35.844

36.856

8.234

9.559

0 5 10 15 20 25 30 35 40

min

PDA Ch1 254nm

Peak#

Ret. Time	Area	Height	Conc.	Unit	Mark	Name
1	2.385	66361	5673	1.140
2	2.566	62661	7905	1.076		V
3	2.942	29148	1771	0.501		V
4	3.307	26660	3087	0.458		V
5	3.534	117348	5258	2.015		V
6	4.414	58706	2205	1.008		V
7	5.348	918271	34403	15.770		V
8	6.261	59676	2179	1.025		V
9	6.783	27163	1178	0.467		V
10	7.168	15467	605	0.266		V
11	8.234	8949	330	0.154		V
12	9.559	4287	208	0.074
13	12.459	5579	213	0.096
14	13.981	1424964	40655	24.472		V
15	24.705	728575	20712	12.513
16	25.134	58695	7673	1.008		V
17	25.537	678950	34243	11.660		V
18	25.818	39216	3841	0.674
19	26.155	95901	7902	1.647
20	26.474	173097	11024	2.973		V
21	26.921	102659	6321	1.763		V
22	27.154	142367	10071	2.445		V

D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH-1-20-3-2019.lcd

3/21/2019 7:04:08 PM Page 1 / 2

Analysis Report

Sample Name :

Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH -1- L3.2-22-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm

Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/21/2019 12:12:11 PM Acquired by : System Administrator Date Processed : 3/21/2019 12:53:13 PM Processed by : System Administrator

mAU

PDA Multi 1 254nm,4nm

25.800

2.524

2.701

3.143

3.451

3.693

5.753

14.763

24.766

27.920

28.244

4.627

7.147

7.797

27 26.590

.127

30.440

30.610

31.781

34.285

36.504

37.408

0 5 10 15 20 25 30 35 40

min

PDA Ch1 254nm

Peak#

Ret. Time	Area	Height	Conc.	Unit	Mark	Name
1	2.524	61215	4820	0.000
2	2.701	71881	6105	0.000		V
3	3.143	17396	1272	0.000		V
4	3.451	28204	2480	0.000		V
5	3.693	121861	4833	0.000		V
6	4.627	53057	1991	0.000		V
7	5.753	1043674	33001	0.000		SV
8	7.147	4348	299	0.000		T
9	7.797	1226	45	0.000		T
10	14.763	1475847	32493	0.000
11	24.766	277649	10236	0.000
12	25.800	3489806	59826	0.000		V
13	26.590	138772	8324	0.000		V
14	27.127	104608	4483	0.000		SV
15	27.920	12013	708	0.000		V
16	28.244	12477	957	0.000		V
17	30.440	55875	4795	0.000
18	30.610	57859	4211	0.000		V
19	31.781	3899	244	0.000
20	34.285	83873	3748	0.000		S
21	36.504	121968	5345	0.000
22	37.408	5642	273	0.000		V

D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH -1- L3.2-22-3-2019.lcd

3/21/2019 7:04:09 PM Page 1 / 2

Analysis Report

Sample Name :

Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH -1- L4-22-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm

Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/21/2019 1:21:33 PM Acquired by : System Administrator Date Processed : 3/21/2019 2:02:35 PM Processed by : System Administrator

mAU

PDA Multi 1 254nm,4nm

25.612

25.723

2.553

2.742

5.918

15.075

24.829

27. 26.625 27.666

155

27.968

28.275

0.035

1.013

3.682

4.655

6.923

30.465

30.647

31.810

34.275

36.471

37.399

0 5 10 15 20 25 30 35 40

min

PDA Ch1 254nm

Peak#

Ret. Time	Area	Height	Conc.	Unit	Mark	Name
1	0.035	5626	464	0.000
2	1.013	3982	188	0.000
3	2.553	65492	4714	0.000
4	2.742	98848	6258	0.000		V
5	3.682	150838	4732	0.000		V
6	4.655	50825	1904	0.000		V
7	5.918	944518	27743	0.000		V
8	6.923	48059	1604	0.000		V
9	15.075	1465971	31450	0.000
10	24.829	329784	10507	0.000
11	25.612	1515321	54151	0.000		V
12	25.723	1490014	54495	0.000		V
13	26.625	131812	9485	0.000		V
14	27.155	95130	4583	0.000		V
15	27.666	6076	534	0.000		V
16	27.968	12281	741	0.000		V
17	28.275	12172	1017	0.000		V
18	30.465	59105	5217	0.000
19	30.647	54430	4255	0.000		V
20	31.810	4673	279	0.000
21	34.275	96732	3850	0.000
22	36.471	114207	5265	0.000

D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH -1- L4-22-3-2019.lcd

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