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3/21/2019 7:04:46 PM Page 1 / 1


Analysis Report


<Sample Information>

Sample Name :

Sample ID :

Data Filename : oxo chuan 6.25ug 19-3-2019.lcd

Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/19/2019 8:15:58 PM Acquired by : System Administrator Date Processed : 3/19/2019 8:36:43 PM Processed by : System Administrator


<Chromatogram>

mAU


PDA Multi 1 254nm,4nm

14.165

12.5


10.0


7.5


5.0


2.595

2.5


2.243

2.475

0.0


0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0

min

<Peak Table>

PDA Ch1 254nm

Peak#

Ret. Time

Area

Height

Conc.

Unit

Mark

Name

1

2.243

3210

348

0.000




2

2.475

3077

408

0.000


V


3

2.595

23768

2617

0.000


V


4

14.165

418469

11975

0.000




Total


448525

15348





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Nghiên cứu thành phần hóa học và đánh giá tác dụng kháng ung thư của thân lá cây củ dòm Stephania dielsiana Y.C. Wu - 37


D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 6.25ug 19-3-2019.lcd

5/3/2019 12:34:40 PM Page 1 / 1


Analysis Report


<Sample Information>

Sample Name :

Sample ID :

Data Filename : oxo chuan 12.5ug 19-3-2019.lcd

Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/19/2019 7:53:40 PM Acquired by : System Administrator Date Processed : 3/19/2019 8:14:25 PM Processed by : System Administrator


<Chromatogram>

mAU


PDA Multi 1 254nm,4nm

14.131

20


15


10


2.589

5


0


0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0

min

<Peak Table>

PDA Ch1 254nm

Peak#

Ret. Time

Area

Height

Conc.

Unit

Mark

Name

1

2.589

20242

2277

0.000




2

14.131

696245

20198

0.000




Total


716486

22475






D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 12.5ug 19-3-2019.lcd

5/3/2019 12:34:37 PM Page 1 / 1


Analysis Report


<Sample Information>

Sample Name :

Sample ID :

Data Filename : oxo chuan 25ug 19-3-2019.lcd

Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/19/2019 7:30:36 PM Acquired by : System Administrator Date Processed : 3/19/2019 7:51:39 PM Processed by : System Administrator


<Chromatogram>

14.111

mAU


PDA Multi 1 254nm,4nm

30


20


10


2.589

3.288

0


0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0

min

<Peak Table>

PDA Ch1 254nm

Peak#

Ret. Time

Area

Height

Conc.

Unit

Mark

Name

1

2.589

18451

2032

0.000




2

3.288

5923

131

0.000




3

14.111

1214153

34814

0.000




Total


1238527

36978






D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 25ug 19-3-2019.lcd

5/3/2019 12:34:32 PM Page 1 / 1


Analysis Report


<Sample Information>

Sample Name :

Sample ID :

Data Filename : oxo chuan 50ug 19-3-2019.lcd

Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/19/2019 7:01:24 PM Acquired by : System Administrator Date Processed : 3/19/2019 7:22:26 PM Processed by : System Administrator


<Chromatogram>

mAU


PDA Multi 1 254nm,4nm

14.069

75



50



25



2.591

3.288

0


0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0

min

<Peak Table>

PDA Ch1 254nm

Peak#

Ret. Time

Area

Height

Conc.

Unit

Mark

Name

1

2.591

13294

1671

0.000




2

3.288

6211

181

0.000




3

14.069

2506725

71991

0.000




Total


2526229

73842






D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 50ug 19-3-2019.lcd

5/3/2019 12:34:40 PM Page 1 / 1


Analysis Report


<Sample Information>

Sample Name :

Sample ID :

Data Filename : oxo chuan 100ug 19-3-2019.lcd

Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/19/2019 6:35:20 PM Acquired by : System Administrator Date Processed : 3/19/2019 6:56:22 PM Processed by : System Administrator


<Chromatogram>

mAU


PDA Multi 1 254nm,4nm

13.725

125


100


75


2.204 2.571

2.675 3.019

3.236

50


0.324

25


0


0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0

min

<Peak Table>

PDA Ch1 254nm

Peak#

Ret. Time

Area

Height

Conc.

Unit

Mark

Name

1

0.324

37725

7640

0.000




2

2.204

1005

151

0.000




3

2.571

4291

1236

0.000




4

2.675

12020

1079

0.000


V


5

3.019

2780

232

0.000




6

3.236

1322

181

0.000


V


7

13.725

4900220

135794

0.000




Total


4959363

146313






D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 100ug 19-3-2019.lcd

Phụ lục 4.3.3. Sắc ký đồ các mẫu thẩm định độ lặp lại


3/21/2019 7:04:14 PM Page 1 / 2


Analysis Report


<Sample Information>

Sample Name : Mau chiet 1 Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH-1-20-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename : oxo-batch-20-03-2019.lcb

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/20/2019 8:19:47 PM Acquired by : System Administrator Date Processed : 3/21/2019 10:33:23 AM Processed by : System Administrator


<Chromatogram>

mAU


PDA Multi 1 254nm,4nm

5.348

13.981

25.818

262.155.5537

26.474

33.615

40


24.705

26.921

27.154

30


2.385

2.566

2.942

3.307

3.534

20


4.414

6.783

7.168

6.261

12.459

25.134

27.734

28.020

28.395

30.059

31.474

35.844

36.856

10


8.234

9.559

0


0 5 10 15 20 25 30 35 40

min

<Peak Table>

PDA Ch1 254nm

Peak#

Ret. Time

Area

Height

Conc.

Unit

Mark

Name

1

2.385

66361

5673

1.140




2

2.566

62661

7905

1.076


V


3

2.942

29148

1771

0.501


V


4

3.307

26660

3087

0.458


V


5

3.534

117348

5258

2.015


V


6

4.414

58706

2205

1.008


V


7

5.348

918271

34403

15.770


V


8

6.261

59676

2179

1.025


V


9

6.783

27163

1178

0.467


V


10

7.168

15467

605

0.266


V


11

8.234

8949

330

0.154


V


12

9.559

4287

208

0.074




13

12.459

5579

213

0.096




14

13.981

1424964

40655

24.472


V


15

24.705

728575

20712

12.513




16

25.134

58695

7673

1.008


V


17

25.537

678950

34243

11.660


V


18

25.818

39216

3841

0.674




19

26.155

95901

7902

1.647




20

26.474

173097

11024

2.973


V


21

26.921

102659

6321

1.763


V


22

27.154

142367

10071

2.445


V



D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH-1-20-3-2019.lcd

3/21/2019 7:04:08 PM Page 1 / 2


Analysis Report


<Sample Information>

Sample Name :

Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH -1- L3.2-22-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm

Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/21/2019 12:12:11 PM Acquired by : System Administrator Date Processed : 3/21/2019 12:53:13 PM Processed by : System Administrator


<Chromatogram>

mAU


PDA Multi 1 254nm,4nm

25.800

50


2.524

2.701

3.143

3.451

3.693

5.753

14.763

24.766

27.920

28.244

25


4.627

7.147

7.797

27 26.590

.127

30.440

30.610

31.781

34.285

36.504

37.408

0


0 5 10 15 20 25 30 35 40

min

<Peak Table>

PDA Ch1 254nm

Peak#

Ret. Time

Area

Height

Conc.

Unit

Mark

Name

1

2.524

61215

4820

0.000




2

2.701

71881

6105

0.000


V


3

3.143

17396

1272

0.000


V


4

3.451

28204

2480

0.000


V


5

3.693

121861

4833

0.000


V


6

4.627

53057

1991

0.000


V


7

5.753

1043674

33001

0.000


SV


8

7.147

4348

299

0.000


T


9

7.797

1226

45

0.000


T


10

14.763

1475847

32493

0.000




11

24.766

277649

10236

0.000




12

25.800

3489806

59826

0.000


V


13

26.590

138772

8324

0.000


V


14

27.127

104608

4483

0.000


SV


15

27.920

12013

708

0.000


V


16

28.244

12477

957

0.000


V


17

30.440

55875

4795

0.000




18

30.610

57859

4211

0.000


V


19

31.781

3899

244

0.000




20

34.285

83873

3748

0.000


S


21

36.504

121968

5345

0.000




22

37.408

5642

273

0.000


V



D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH -1- L3.2-22-3-2019.lcd

3/21/2019 7:04:09 PM Page 1 / 2


Analysis Report


<Sample Information>

Sample Name :

Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH -1- L4-22-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm

Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/21/2019 1:21:33 PM Acquired by : System Administrator Date Processed : 3/21/2019 2:02:35 PM Processed by : System Administrator


<Chromatogram>

mAU



PDA Multi 1 254nm,4nm

25.612

25.723

50



2.553

2.742

5.918

15.075

24.829

27. 26.625 27.666

155

27.968

28.275

25



0.035

1.013

3.682

4.655

6.923

30.465

30.647

31.810

34.275

36.471

37.399

0


0 5 10 15 20 25 30 35 40

min

<Peak Table>

PDA Ch1 254nm

Peak#

Ret. Time

Area

Height

Conc.

Unit

Mark

Name

1

0.035

5626

464

0.000




2

1.013

3982

188

0.000




3

2.553

65492

4714

0.000




4

2.742

98848

6258

0.000


V


5

3.682

150838

4732

0.000


V


6

4.655

50825

1904

0.000


V


7

5.918

944518

27743

0.000


V


8

6.923

48059

1604

0.000


V


9

15.075

1465971

31450

0.000




10

24.829

329784

10507

0.000




11

25.612

1515321

54151

0.000


V


12

25.723

1490014

54495

0.000


V


13

26.625

131812

9485

0.000


V


14

27.155

95130

4583

0.000


V


15

27.666

6076

534

0.000


V


16

27.968

12281

741

0.000


V


17

28.275

12172

1017

0.000


V


18

30.465

59105

5217

0.000




19

30.647

54430

4255

0.000


V


20

31.810

4673

279

0.000




21

34.275

96732

3850

0.000




22

36.471

114207

5265

0.000





D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH -1- L4-22-3-2019.lcd

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