3/21/2019 7:04:46 PM Page 1 / 1
Analysis Report
<Sample Information>
Sample Name :
Sample ID :
Data Filename : oxo chuan 6.25ug 19-3-2019.lcd
Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :
Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL
Date Acquired : 3/19/2019 8:15:58 PM Acquired by : System Administrator Date Processed : 3/19/2019 8:36:43 PM Processed by : System Administrator
<Chromatogram>
mAU
PDA Multi 1 254nm,4nm
14.165
12.5
10.0
7.5
5.0
2.595
2.5
2.243
2.475
0.0
0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0
min
<Peak Table>
PDA Ch1 254nm
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 2.243 | 3210 | 348 | 0.000 | |||
2 | 2.475 | 3077 | 408 | 0.000 | V | ||
3 | 2.595 | 23768 | 2617 | 0.000 | V | ||
4 | 14.165 | 418469 | 11975 | 0.000 | |||
Total | 448525 | 15348 |
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D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 6.25ug 19-3-2019.lcd
5/3/2019 12:34:40 PM Page 1 / 1
Analysis Report
<Sample Information>
Sample Name :
Sample ID :
Data Filename : oxo chuan 12.5ug 19-3-2019.lcd
Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :
Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL
Date Acquired : 3/19/2019 7:53:40 PM Acquired by : System Administrator Date Processed : 3/19/2019 8:14:25 PM Processed by : System Administrator
<Chromatogram>
mAU
PDA Multi 1 254nm,4nm
14.131
20
15
10
2.589
5
0
0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0
min
<Peak Table>
PDA Ch1 254nm
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 2.589 | 20242 | 2277 | 0.000 | |||
2 | 14.131 | 696245 | 20198 | 0.000 | |||
Total | 716486 | 22475 |
D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 12.5ug 19-3-2019.lcd
5/3/2019 12:34:37 PM Page 1 / 1
Analysis Report
<Sample Information>
Sample Name :
Sample ID :
Data Filename : oxo chuan 25ug 19-3-2019.lcd
Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :
Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL
Date Acquired : 3/19/2019 7:30:36 PM Acquired by : System Administrator Date Processed : 3/19/2019 7:51:39 PM Processed by : System Administrator
<Chromatogram>
14.111
mAU
PDA Multi 1 254nm,4nm
30
20
10
2.589
3.288
0
0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0
min
<Peak Table>
PDA Ch1 254nm
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 2.589 | 18451 | 2032 | 0.000 | |||
2 | 3.288 | 5923 | 131 | 0.000 | |||
3 | 14.111 | 1214153 | 34814 | 0.000 | |||
Total | 1238527 | 36978 |
D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 25ug 19-3-2019.lcd
5/3/2019 12:34:32 PM Page 1 / 1
Analysis Report
<Sample Information>
Sample Name :
Sample ID :
Data Filename : oxo chuan 50ug 19-3-2019.lcd
Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :
Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL
Date Acquired : 3/19/2019 7:01:24 PM Acquired by : System Administrator Date Processed : 3/19/2019 7:22:26 PM Processed by : System Administrator
<Chromatogram>
mAU
PDA Multi 1 254nm,4nm
14.069
75
50
25
2.591
3.288
0
0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0
min
<Peak Table>
PDA Ch1 254nm
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 2.591 | 13294 | 1671 | 0.000 | |||
2 | 3.288 | 6211 | 181 | 0.000 | |||
3 | 14.069 | 2506725 | 71991 | 0.000 | |||
Total | 2526229 | 73842 |
D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 50ug 19-3-2019.lcd
5/3/2019 12:34:40 PM Page 1 / 1
Analysis Report
<Sample Information>
Sample Name :
Sample ID :
Data Filename : oxo chuan 100ug 19-3-2019.lcd
Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :
Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL
Date Acquired : 3/19/2019 6:35:20 PM Acquired by : System Administrator Date Processed : 3/19/2019 6:56:22 PM Processed by : System Administrator
<Chromatogram>
mAU
PDA Multi 1 254nm,4nm
13.725
125
100
75
2.204 2.571
2.675 3.019
3.236
50
0.324
25
0
0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0
min
<Peak Table>
PDA Ch1 254nm
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 0.324 | 37725 | 7640 | 0.000 | |||
2 | 2.204 | 1005 | 151 | 0.000 | |||
3 | 2.571 | 4291 | 1236 | 0.000 | |||
4 | 2.675 | 12020 | 1079 | 0.000 | V | ||
5 | 3.019 | 2780 | 232 | 0.000 | |||
6 | 3.236 | 1322 | 181 | 0.000 | V | ||
7 | 13.725 | 4900220 | 135794 | 0.000 | |||
Total | 4959363 | 146313 |
D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 100ug 19-3-2019.lcd
Phụ lục 4.3.3. Sắc ký đồ các mẫu thẩm định độ lặp lại
3/21/2019 7:04:14 PM Page 1 / 2
Analysis Report
<Sample Information>
Sample Name : Mau chiet 1 Sample ID :
Data Filename : Mau chiet 0.5 g trong 50ml MeOH-1-20-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename : oxo-batch-20-03-2019.lcb
Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL
Date Acquired : 3/20/2019 8:19:47 PM Acquired by : System Administrator Date Processed : 3/21/2019 10:33:23 AM Processed by : System Administrator
<Chromatogram>
mAU
PDA Multi 1 254nm,4nm
5.348
13.981
25.818
262.155.5537
26.474
33.615
40
24.705
26.921
27.154
30
2.385
2.566
2.942
3.307
3.534
20
4.414
6.783
7.168
6.261
12.459
25.134
27.734
28.020
28.395
30.059
31.474
35.844
36.856
10
8.234
9.559
0
0 5 10 15 20 25 30 35 40
min
<Peak Table>
PDA Ch1 254nm
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 2.385 | 66361 | 5673 | 1.140 | |||
2 | 2.566 | 62661 | 7905 | 1.076 | V | ||
3 | 2.942 | 29148 | 1771 | 0.501 | V | ||
4 | 3.307 | 26660 | 3087 | 0.458 | V | ||
5 | 3.534 | 117348 | 5258 | 2.015 | V | ||
6 | 4.414 | 58706 | 2205 | 1.008 | V | ||
7 | 5.348 | 918271 | 34403 | 15.770 | V | ||
8 | 6.261 | 59676 | 2179 | 1.025 | V | ||
9 | 6.783 | 27163 | 1178 | 0.467 | V | ||
10 | 7.168 | 15467 | 605 | 0.266 | V | ||
11 | 8.234 | 8949 | 330 | 0.154 | V | ||
12 | 9.559 | 4287 | 208 | 0.074 | |||
13 | 12.459 | 5579 | 213 | 0.096 | |||
14 | 13.981 | 1424964 | 40655 | 24.472 | V | ||
15 | 24.705 | 728575 | 20712 | 12.513 | |||
16 | 25.134 | 58695 | 7673 | 1.008 | V | ||
17 | 25.537 | 678950 | 34243 | 11.660 | V | ||
18 | 25.818 | 39216 | 3841 | 0.674 | |||
19 | 26.155 | 95901 | 7902 | 1.647 | |||
20 | 26.474 | 173097 | 11024 | 2.973 | V | ||
21 | 26.921 | 102659 | 6321 | 1.763 | V | ||
22 | 27.154 | 142367 | 10071 | 2.445 | V |
D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH-1-20-3-2019.lcd
3/21/2019 7:04:08 PM Page 1 / 2
Analysis Report
<Sample Information>
Sample Name :
Sample ID :
Data Filename : Mau chiet 0.5 g trong 50ml MeOH -1- L3.2-22-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm
Batch Filename :
Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL
Date Acquired : 3/21/2019 12:12:11 PM Acquired by : System Administrator Date Processed : 3/21/2019 12:53:13 PM Processed by : System Administrator
<Chromatogram>
mAU
PDA Multi 1 254nm,4nm
25.800
50
2.524
2.701
3.143
3.451
3.693
5.753
14.763
24.766
27.920
28.244
25
4.627
7.147
7.797
27 26.590
.127
30.440
30.610
31.781
34.285
36.504
37.408
0
0 5 10 15 20 25 30 35 40
min
<Peak Table>
PDA Ch1 254nm
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 2.524 | 61215 | 4820 | 0.000 | |||
2 | 2.701 | 71881 | 6105 | 0.000 | V | ||
3 | 3.143 | 17396 | 1272 | 0.000 | V | ||
4 | 3.451 | 28204 | 2480 | 0.000 | V | ||
5 | 3.693 | 121861 | 4833 | 0.000 | V | ||
6 | 4.627 | 53057 | 1991 | 0.000 | V | ||
7 | 5.753 | 1043674 | 33001 | 0.000 | SV | ||
8 | 7.147 | 4348 | 299 | 0.000 | T | ||
9 | 7.797 | 1226 | 45 | 0.000 | T | ||
10 | 14.763 | 1475847 | 32493 | 0.000 | |||
11 | 24.766 | 277649 | 10236 | 0.000 | |||
12 | 25.800 | 3489806 | 59826 | 0.000 | V | ||
13 | 26.590 | 138772 | 8324 | 0.000 | V | ||
14 | 27.127 | 104608 | 4483 | 0.000 | SV | ||
15 | 27.920 | 12013 | 708 | 0.000 | V | ||
16 | 28.244 | 12477 | 957 | 0.000 | V | ||
17 | 30.440 | 55875 | 4795 | 0.000 | |||
18 | 30.610 | 57859 | 4211 | 0.000 | V | ||
19 | 31.781 | 3899 | 244 | 0.000 | |||
20 | 34.285 | 83873 | 3748 | 0.000 | S | ||
21 | 36.504 | 121968 | 5345 | 0.000 | |||
22 | 37.408 | 5642 | 273 | 0.000 | V |
D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH -1- L3.2-22-3-2019.lcd
3/21/2019 7:04:09 PM Page 1 / 2
Analysis Report
<Sample Information>
Sample Name :
Sample ID :
Data Filename : Mau chiet 0.5 g trong 50ml MeOH -1- L4-22-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm
Batch Filename :
Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL
Date Acquired : 3/21/2019 1:21:33 PM Acquired by : System Administrator Date Processed : 3/21/2019 2:02:35 PM Processed by : System Administrator
<Chromatogram>
mAU
PDA Multi 1 254nm,4nm
25.612
25.723
50
2.553
2.742
5.918
15.075
24.829
27. 26.625 27.666
155
27.968
28.275
25
0.035
1.013
3.682
4.655
6.923
30.465
30.647
31.810
34.275
36.471
37.399
0
0 5 10 15 20 25 30 35 40
min
<Peak Table>
PDA Ch1 254nm
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 0.035 | 5626 | 464 | 0.000 | |||
2 | 1.013 | 3982 | 188 | 0.000 | |||
3 | 2.553 | 65492 | 4714 | 0.000 | |||
4 | 2.742 | 98848 | 6258 | 0.000 | V | ||
5 | 3.682 | 150838 | 4732 | 0.000 | V | ||
6 | 4.655 | 50825 | 1904 | 0.000 | V | ||
7 | 5.918 | 944518 | 27743 | 0.000 | V | ||
8 | 6.923 | 48059 | 1604 | 0.000 | V | ||
9 | 15.075 | 1465971 | 31450 | 0.000 | |||
10 | 24.829 | 329784 | 10507 | 0.000 | |||
11 | 25.612 | 1515321 | 54151 | 0.000 | V | ||
12 | 25.723 | 1490014 | 54495 | 0.000 | V | ||
13 | 26.625 | 131812 | 9485 | 0.000 | V | ||
14 | 27.155 | 95130 | 4583 | 0.000 | V | ||
15 | 27.666 | 6076 | 534 | 0.000 | V | ||
16 | 27.968 | 12281 | 741 | 0.000 | V | ||
17 | 28.275 | 12172 | 1017 | 0.000 | V | ||
18 | 30.465 | 59105 | 5217 | 0.000 | |||
19 | 30.647 | 54430 | 4255 | 0.000 | V | ||
20 | 31.810 | 4673 | 279 | 0.000 | |||
21 | 34.275 | 96732 | 3850 | 0.000 | |||
22 | 36.471 | 114207 | 5265 | 0.000 |
D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH -1- L4-22-3-2019.lcd