Sắc Ký Đồ Các Mẫu Thẩm Định Độ Đúng

3/21/2019 7:04:09 PM Page 1 / 2

Analysis Report

Sample Name :

Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH -1- L5-22-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm

Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/21/2019 2:33:31 PM Acquired by : System Administrator Date Processed : 3/21/2019 3:24:33 PM Processed by : System Administrator

25.732

mAU

PDA Multi 1 254nm,4nm

5.725

14.400

2.472

2.645

3.062

3.378

3.645

26.564

27.113

27.985

28.238

4.566

7.008

13.131

30.436

31.639

34.101

36.218

37.106

42.527

46.087

46.332

0 10 20 30 40 50

min

PDA Ch1 254nm

Peak#

Ret. Time	Area	Height	Conc.	Unit	Mark	Name
1	2.472	61966	4904	0.000
2	2.645	71654	6520	0.000		V
3	3.062	17740	1337	0.000		V
4	3.378	31517	2513	0.000		V
5	3.645	125977	4972	0.000		V
6	4.566	61275	2128	0.000		V
7	5.725	1034714	33587	0.000		SV
8	7.008	4271	262	0.000		T
9	13.131	1253	70	0.000
10	14.400	1447025	32237	0.000		V
11	25.732	3474187	60001	0.000
12	26.564	129841	9410	0.000		V
13	27.113	103145	4877	0.000		SV
14	27.985	11969	694	0.000		V
15	28.238	10494	897	0.000		V
16	30.436	117703	5333	0.000
17	31.639	3938	253	0.000
18	34.101	79758	3726	0.000		S
19	36.218	119136	5137	0.000
20	37.106	8208	342	0.000		V
21	42.527	41810	1307	0.000
22	46.087	36952	2475	0.000

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D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH -1- L5-22-3-2019.lcd

3/21/2019 7:04:10 PM Page 1 / 2

Analysis Report

Sample Name :

Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH -1- L6-22-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm

Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/21/2019 3:26:30 PM Acquired by : System Administrator Date Processed : 3/21/2019 4:17:33 PM Processed by : System Administrator

mAU

PDA Multi 1 254nm,4nm

25.709

5.635

14.209

2.462

2.637

3.083

3.357

4.526 3.624

26.569

27.099

27.966

28.245

36.150

5.163

6.954

29.523

30.460

31.634

34.057

34.773

39.178

42.379

46.096

46.361

0 10 20 30 40 50

min

PDA Ch1 254nm

Peak#

Ret. Time	Area	Height	Conc.	Unit	Mark	Name
1	2.462	60832	4927	0.000
2	2.637	69184	6583	0.000		V
3	3.083	18437	1248	0.000		V
4	3.357	29678	2474	0.000		V
5	3.624	120118	4987	0.000		V
6	4.526	56323	2049	0.000		V
7	5.163	24673	1617	0.000		V
8	5.635	981435	33610	0.000		SV
9	6.954	4330	316	0.000		T
10	14.209	1414563	32250	0.000
11	25.709	3839197	73047	0.000
12	26.569	140745	9762	0.000		V
13	27.099	123744	5362	0.000		SV
14	27.966	15187	880	0.000		V
15	28.245	12292	928	0.000		V
16	29.523	1643	145	0.000
17	30.460	113882	5349	0.000
18	31.634	4327	249	0.000
19	34.057	86463	4001	0.000
20	34.773	3859	211	0.000		V
21	36.150	108575	4889	0.000
22	39.178	80171	950	0.000

D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH -1- L6-22-3-2019.lcd

3/21/2019 7:04:15 PM Page 1 / 2

Analysis Report

Sample Name : Mauchiet 1 intra Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH-1-intra-20-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm

Batch Filename : oxo-batch-20-03-2019.lcb

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/21/2019 1:28:18 AM Acquired by : System Administrator Date Processed : 3/21/2019 12:55:21 PM Processed by : System Administrator

mAU

PDA Multi 1 254nm,4nm

5.626

14.532

27.747

27.975

2.402

2.573

2.962

3.332

3.583

24.235

24.320

24.549

24.759

24.957

25.167

25.430

25.621

25.809

25.921

26.060

26.228

30.029 26.510

31.467

4.500

6.644

6.965

33.585

35.858

36.852

10.166

26.955

27.029

0 5 10 15 20 25 30 35 40

min

PDA Ch1 254nm

Peak#

Ret. Time	Area	Height	Conc.	Unit	Mark	Name
1	2.402	67506	5817	1.891		V
2	2.573	61431	7313	1.721		V
3	2.962	27971	1721	0.784		V
4	3.332	27060	2854	0.758		V
5	3.583	115026	4946	3.223		V
6	4.500	49723	1987	1.393		V
7	5.626	939365	33412	26.321		SV
8	6.644	6022	406	0.169		TV
9	6.965	8627	490	0.242		TV
10	10.166	3386	188	0.095
11	14.532	1407767	39192	39.445
12	24.235	5381	791	0.151
13	24.320	5063	1174	0.142		V
14	24.549	46373	5401	1.299		V
15	24.759	61019	6586	1.710		V
16	24.957	52288	4396	1.465		V
17	25.167	30661	2717	0.859		V
18	25.430	17601	2698	0.493		V
19	25.621	10443	1722	0.293		V
20	25.809	20653	2146	0.579		V
21	25.921	6640	1491	0.186		V
22	26.060	10241	1085	0.287		V

D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH-1-intra-20-3-2019.lcd

Phụ lục 4.3.4. Sắc ký đồ các mẫu thẩm định độ đúng

5/3/2019 12:34:56 PM Page 1 / 1

Analysis Report

Sample Name :

Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH thêm 120% chuan22-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm

Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/21/2019 5:27:25 PM Acquired by : System Administrator Date Processed : 3/22/2019 11:16:30 AM Processed by : System Administrator

13.946

mAU

PDA Multi 1 254nm,4nm

0 10 20 30 40 50

min

PDA Ch1 254nm

Peak#

Ret. Time	Area	Height	Conc.	Unit	Mark	Name
1	13.946	3009994	67919	0.000		M
Total		3009994	67919

D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH thêm 120% chuan22-3-2019.lcd

5/3/2019 12:34:59 PM Page 1 / 2

Analysis Report

Sample Name :

Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH thêm 100% l2chuan22-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm

Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/21/2019 6:22:17 PM Acquired by : System Administrator Date Processed : 3/21/2019 7:13:20 PM Processed by : System Administrator

mAU

PDA Multi 1 254nm,4nm

30.365

150

25.675

100

2.436

2.613

3.021

3.312

3.577

5.467

13.870

27.659

27.952

31.520

31.955

33.925

4.454

6.199

6.816

26.524

27.059

29.453

29.707

32.574

35.986

42.114

46.104

46.392

0 10 20 30 40 50

min

PDA Ch1 254nm

Peak#

Ret. Time	Area	Height	Conc.	Unit	Mark	Name
1	2.436	60251	4891	0.000
2	2.613	71933	6362	0.000		V
3	3.021	17136	1274	0.000		V
4	3.312	28826	2479	0.000		V
5	3.577	113817	4778	0.000		V
6	4.454	53952	1935	0.000		V
7	5.467	980322	33596	0.000		SV
8	6.199	5937	386	0.000		T
9	6.816	1586	159	0.000		T
10	13.870	2388696	55838	0.000
11	25.675	3706074	68034	0.000
12	26.524	139454	10621	0.000		V
13	27.059	126240	5768	0.000		V
14	27.659	5878	546	0.000		V
15	27.952	28118	1255	0.000		V
16	29.453	2160	182	0.000
17	29.707	1085	117	0.000		V
18	30.365	2029093	144158	0.000
19	31.520	2589	199	0.000		V
20	31.955	2695	171	0.000
21	32.574	2387	139	0.000
22	33.925	202519	10044	0.000

D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH thêm 100% l2chuan22-3-2019.lcd

5/3/2019 12:34:55 PM Page 1 / 2

Analysis Report

Sample Name :

Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH thêm 80% l2chuan22-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm

Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/21/2019 7:19:15 PM Acquired by : System Administrator Date Processed : 3/21/2019 8:10:17 PM Processed by : System Administrator

mAU

PDA Multi 1 254nm,4nm

5.267

12.476

25.639

2.408

2.583

2.997

3.271

3.527

5.879

6.400

30.264

4.384

7.308

8.491

26.473

27.023

27.900

31.416

31.830

33.790

35.814

41.857

46.106

46.405

0 10 20 30 40 50

min

PDA Ch1 254nm

Peak#

Ret. Time	Area	Height	Conc.	Unit	Mark	Name
1	2.408	66155	5329	0.000
2	2.583	73382	6821	0.000		V
3	2.997	20538	1454	0.000		V
4	3.271	32059	2764	0.000		V
5	3.527	122761	5254	0.000		V
6	4.384	62822	2286	0.000		V
7	5.267	1039195	48127	0.000		SV
8	5.879	14062	1054	0.000		T
9	6.400	2672	146	0.000		T
10	7.308	4559	263	0.000		T
11	8.491	5088	240	0.000
12	12.476	2378018	57882	0.000
13	25.639	3410129	58463	0.000
14	26.473	139190	9723	0.000		V
15	27.023	99875	4836	0.000		V
16	27.900	17693	934	0.000
17	30.264	454125	29388	0.000
18	31.416	4932	279	0.000
19	31.830	5890	316	0.000		V
20	33.790	120889	5286	0.000
21	35.814	109541	4942	0.000
22	41.857	31651	1170	0.000

D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH thêm 80% l2chuan22-3-2019.lcd

PHỤ LỤC 5.

KẾT QUẢ ĐÁNH GIÁ TÁC DỤNG GÂY ĐỘC TẾ BÀO IN VITRO

PHỤ LỤC 5.

KẾT QUẢ ĐÁNH GIÁ TÁC DỤNG GÂY ĐỘC TẾ BÀO IN VITRO

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