Sắc Ký Đồ Các Mẫu Thẩm Định Độ Đúng

3/21/2019 7:04:09 PM Page 1 / 2


Analysis Report


<Sample Information>

Sample Name :

Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH -1- L5-22-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm

Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/21/2019 2:33:31 PM Acquired by : System Administrator Date Processed : 3/21/2019 3:24:33 PM Processed by : System Administrator


<Chromatogram>

25.732

mAU


PDA Multi 1 254nm,4nm

5.725

14.400

50


2.472

2.645

3.062

3.378

3.645

26.564

27.113

27.985

28.238

25


4.566

7.008

13.131

30.436

31.639

34.101

36.218

37.106

42.527

46.087

46.332

0


0 10 20 30 40 50

min

<Peak Table>

PDA Ch1 254nm

Peak#

Ret. Time

Area

Height

Conc.

Unit

Mark

Name

1

2.472

61966

4904

0.000




2

2.645

71654

6520

0.000


V


3

3.062

17740

1337

0.000


V


4

3.378

31517

2513

0.000


V


5

3.645

125977

4972

0.000


V


6

4.566

61275

2128

0.000


V


7

5.725

1034714

33587

0.000


SV


8

7.008

4271

262

0.000


T


9

13.131

1253

70

0.000




10

14.400

1447025

32237

0.000


V


11

25.732

3474187

60001

0.000




12

26.564

129841

9410

0.000


V


13

27.113

103145

4877

0.000


SV


14

27.985

11969

694

0.000


V


15

28.238

10494

897

0.000


V


16

30.436

117703

5333

0.000




17

31.639

3938

253

0.000




18

34.101

79758

3726

0.000


S


19

36.218

119136

5137

0.000




20

37.106

8208

342

0.000


V


21

42.527

41810

1307

0.000




22

46.087

36952

2475

0.000




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Nghiên cứu thành phần hóa học và đánh giá tác dụng kháng ung thư của thân lá cây củ dòm Stephania dielsiana Y.C. Wu - 38


D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH -1- L5-22-3-2019.lcd

3/21/2019 7:04:10 PM Page 1 / 2


Analysis Report


<Sample Information>

Sample Name :

Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH -1- L6-22-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm

Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/21/2019 3:26:30 PM Acquired by : System Administrator Date Processed : 3/21/2019 4:17:33 PM Processed by : System Administrator


<Chromatogram>

mAU


PDA Multi 1 254nm,4nm

25.709

75



5.635

14.209

50



2.462

2.637

3.083

3.357

4.526 3.624

26.569

27.099

27.966

28.245

36.150

25



5.163

6.954

29.523

30.460

31.634

34.057

34.773

39.178

42.379

46.096

46.361

0


0 10 20 30 40 50

min

<Peak Table>

PDA Ch1 254nm

Peak#

Ret. Time

Area

Height

Conc.

Unit

Mark

Name

1

2.462

60832

4927

0.000




2

2.637

69184

6583

0.000


V


3

3.083

18437

1248

0.000


V


4

3.357

29678

2474

0.000


V


5

3.624

120118

4987

0.000


V


6

4.526

56323

2049

0.000


V


7

5.163

24673

1617

0.000


V


8

5.635

981435

33610

0.000


SV


9

6.954

4330

316

0.000


T


10

14.209

1414563

32250

0.000




11

25.709

3839197

73047

0.000




12

26.569

140745

9762

0.000


V


13

27.099

123744

5362

0.000


SV


14

27.966

15187

880

0.000


V


15

28.245

12292

928

0.000


V


16

29.523

1643

145

0.000




17

30.460

113882

5349

0.000




18

31.634

4327

249

0.000




19

34.057

86463

4001

0.000




20

34.773

3859

211

0.000


V


21

36.150

108575

4889

0.000




22

39.178

80171

950

0.000





D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH -1- L6-22-3-2019.lcd


3/21/2019 7:04:15 PM Page 1 / 2


Analysis Report


<Sample Information>

Sample Name : Mauchiet 1 intra Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH-1-intra-20-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm

Batch Filename : oxo-batch-20-03-2019.lcb

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/21/2019 1:28:18 AM Acquired by : System Administrator Date Processed : 3/21/2019 12:55:21 PM Processed by : System Administrator


<Chromatogram>

mAU


PDA Multi 1 254nm,4nm

5.626

14.532

40


27.747

27.975

30


2.402

2.573

2.962

3.332

3.583

24.235

24.320

24.549

24.759

24.957

25.167

25.430

25.621

25.809

25.921

26.060

26.228

30.029 26.510

31.467

20


4.500

6.644

6.965

33.585

35.858

36.852

10


10.166

26.955

27.029

0



0 5 10 15 20 25 30 35 40

min

<Peak Table>

PDA Ch1 254nm

Peak#

Ret. Time

Area

Height

Conc.

Unit

Mark

Name

1

2.402

67506

5817

1.891


V


2

2.573

61431

7313

1.721


V


3

2.962

27971

1721

0.784


V


4

3.332

27060

2854

0.758


V


5

3.583

115026

4946

3.223


V


6

4.500

49723

1987

1.393


V


7

5.626

939365

33412

26.321


SV


8

6.644

6022

406

0.169


TV


9

6.965

8627

490

0.242


TV


10

10.166

3386

188

0.095




11

14.532

1407767

39192

39.445




12

24.235

5381

791

0.151




13

24.320

5063

1174

0.142


V


14

24.549

46373

5401

1.299


V


15

24.759

61019

6586

1.710


V


16

24.957

52288

4396

1.465


V


17

25.167

30661

2717

0.859


V


18

25.430

17601

2698

0.493


V


19

25.621

10443

1722

0.293


V


20

25.809

20653

2146

0.579


V


21

25.921

6640

1491

0.186


V


22

26.060

10241

1085

0.287


V



D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH-1-intra-20-3-2019.lcd

Phụ lục 4.3.4. Sắc ký đồ các mẫu thẩm định độ đúng


5/3/2019 12:34:56 PM Page 1 / 1


Analysis Report


<Sample Information>

Sample Name :

Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH thêm 120% chuan22-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm

Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/21/2019 5:27:25 PM Acquired by : System Administrator Date Processed : 3/22/2019 11:16:30 AM Processed by : System Administrator


<Chromatogram>

13.946

mAU


PDA Multi 1 254nm,4nm

50


25


0


0 10 20 30 40 50

min

<Peak Table>

PDA Ch1 254nm

Peak#

Ret. Time

Area

Height

Conc.

Unit

Mark

Name

1

13.946

3009994

67919

0.000


M


Total


3009994

67919






D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH thêm 120% chuan22-3-2019.lcd


5/3/2019 12:34:59 PM Page 1 / 2


Analysis Report


<Sample Information>

Sample Name :

Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH thêm 100% l2chuan22-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm

Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/21/2019 6:22:17 PM Acquired by : System Administrator Date Processed : 3/21/2019 7:13:20 PM Processed by : System Administrator


<Chromatogram>

mAU

PDA Multi 1 254nm,4nm

30.365

150



25.675

100



2.436

2.613

3.021

3.312

3.577

5.467

13.870

27.659

27.952

31.520

31.955

33.925

50



4.454

6.199

6.816

26.524

27.059

29.453

29.707

32.574

35.986

42.114

46.104

46.392

0


0 10 20 30 40 50

min

<Peak Table>

PDA Ch1 254nm

Peak#

Ret. Time

Area

Height

Conc.

Unit

Mark

Name

1

2.436

60251

4891

0.000




2

2.613

71933

6362

0.000


V


3

3.021

17136

1274

0.000


V


4

3.312

28826

2479

0.000


V


5

3.577

113817

4778

0.000


V


6

4.454

53952

1935

0.000


V


7

5.467

980322

33596

0.000


SV


8

6.199

5937

386

0.000


T


9

6.816

1586

159

0.000


T


10

13.870

2388696

55838

0.000




11

25.675

3706074

68034

0.000




12

26.524

139454

10621

0.000


V


13

27.059

126240

5768

0.000


V


14

27.659

5878

546

0.000


V


15

27.952

28118

1255

0.000


V


16

29.453

2160

182

0.000




17

29.707

1085

117

0.000


V


18

30.365

2029093

144158

0.000




19

31.520

2589

199

0.000


V


20

31.955

2695

171

0.000




21

32.574

2387

139

0.000




22

33.925

202519

10044

0.000





D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH thêm 100% l2chuan22-3-2019.lcd

5/3/2019 12:34:55 PM Page 1 / 2


Analysis Report


<Sample Information>

Sample Name :

Sample ID :

Data Filename : Mau chiet 0.5 g trong 50ml MeOH thêm 80% l2chuan22-3-2019.lcd Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm

Batch Filename :

Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL

Date Acquired : 3/21/2019 7:19:15 PM Acquired by : System Administrator Date Processed : 3/21/2019 8:10:17 PM Processed by : System Administrator


<Chromatogram>

mAU


PDA Multi 1 254nm,4nm

5.267

12.476

25.639

50


2.408

2.583

2.997

3.271

3.527

5.879

6.400

30.264

25


4.384

7.308

8.491

26.473

27.023

27.900

31.416

31.830

33.790

35.814

41.857

46.106

46.405

0


0 10 20 30 40 50

min

<Peak Table>

PDA Ch1 254nm

Peak#

Ret. Time

Area

Height

Conc.

Unit

Mark

Name

1

2.408

66155

5329

0.000




2

2.583

73382

6821

0.000


V


3

2.997

20538

1454

0.000


V


4

3.271

32059

2764

0.000


V


5

3.527

122761

5254

0.000


V


6

4.384

62822

2286

0.000


V


7

5.267

1039195

48127

0.000


SV


8

5.879

14062

1054

0.000


T


9

6.400

2672

146

0.000


T


10

7.308

4559

263

0.000


T


11

8.491

5088

240

0.000




12

12.476

2378018

57882

0.000




13

25.639

3410129

58463

0.000




14

26.473

139190

9723

0.000


V


15

27.023

99875

4836

0.000


V


16

27.900

17693

934

0.000




17

30.264

454125

29388

0.000




18

31.416

4932

279

0.000




19

31.830

5890

316

0.000


V


20

33.790

120889

5286

0.000




21

35.814

109541

4942

0.000




22

41.857

31651

1170

0.000





D:HLSONthao-diemoxo chuan 19-3-2019Mau chiet 0.5 g trong 50ml MeOH thêm 80% l2chuan22-3-2019.lcd


PHỤ LỤC 5.

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