7/22/2022 3:39:37 PM Page 1 / 1
Analysis Report
<Sample Information>
: L3.1 | |||
Sample ID | : L3.1 | ||
Data Filename | : L3.1.lcd | ||
Method Filename | : 21-12-01 ÐL oxo trong DL.lcm | ||
Batch Filename | : batch khao sat so lan chiet 2.lcb | ||
Vial # | : 1-9 | Sample Type | : Unknown |
Injection Volume | : 20 uL | ||
Date Acquired | : 08/06/2022 14:09:02 | Acquired by | : System Administrator |
Date Processed | : 08/06/2022 14:34:05 | Processed by | : System Administrator |
Có thể bạn quan tâm!
-
Hợp Chất Sd10: Benzyl Β-D-Glucopyranosid -
Hợp Chất Sd11: (6R,9S)-Roseosid -
Sắc Ký Đồ Các Mẫu Khảo Sát Phương Pháp Xử Lý Mẫu -
Sắc Ký Đồ Các Mẫu Thẩm Định Phương Pháp Phân Tích -
Sắc Ký Đồ Các Mẫu Thẩm Định Độ Lặp Lại -
Sắc Ký Đồ Các Mẫu Thẩm Định Độ Đúng
Xem toàn bộ 368 trang tài liệu này.
<Chromatogram>
mAU
Chiet lan 3
PDA Multi 1 254nm,4nm
14.813
5.0
5.591
20.696
2.5
7.938
0.0
0 5 10 15 20
<Peak Table>
PDA Ch1 254nm
min
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 5.591 | 52262 | 1966 | 0.000 | |||
2 | 7.938 | 9209 | 334 | 0.000 | |||
3 | 14.813 | 220859 | 6438 | 0.000 | |||
4 | 20.696 | 14891 | 335 | 0.000 | SV | ||
Total | 297221 | 9073 |
D:co thuanoxostephanin22-06-08L3.1.lcd
SKĐ cắn chiết lần 3 (hoà tan lại trong MeOH)
7/22/2022 3:41:15 PM Page 1 / 1
Analysis Report
<Sample Information>
: L4.1 | |||
Sample ID | : L4.1 | ||
Data Filename | : L4.1.lcd | ||
Method Filename | : 21-12-01 ÐL oxo trong DL.lcm | ||
Batch Filename | : batch khao sat so lan chiet 2.lcb | ||
Vial # | : 1-12 | Sample Type | : Unknown |
Injection Volume | : 20 uL | ||
Date Acquired | : 08/06/2022 15:51:16 | Acquired by | : System Administrator |
Date Processed | : 08/06/2022 16:16:19 | Processed by | : System Administrator |
<Chromatogram>
14.838
mAU
Chiet lan 4
PDA Multi 1 254nm,4nm
5.593
1
7.961
0
-1
0 5 10 15 20
<Peak Table>
PDA Ch1 254nm
min
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 5.593 | 19783 | 738 | 0.000 | |||
2 | 7.961 | 1305 | 107 | 0.000 | V | ||
3 | 14.838 | 59133 | 1729 | 0.000 | |||
Total | 80220 | 2574 |
D:co thuanoxostephanin22-06-08L4.1.lcd
SKĐ cắn chiết lần 4 (hoà tan lại trong MeOH)
Phụ lục 4.2.2. Sắc ký đồ các mẫu khảo sát lượng dung môi chiết
7/22/2022 3:32:50 PM Page 1 / 1
Analysis Report
<Sample Information>
Sample Name : 25 ml Sample ID : 25 ml Data Filename : 25 ml.lcd
Method Filename : 21-12-01 ÐL oxo trong DL.lcm Batch Filename : batch khao sat luong DM.lcb
Vial # : 1-6 Sample Type : Unknown Injection Volume : 20 uL
Date Acquired : 10/06/2022 14:57:28 Acquired by : System Administrator Date Processed : 10/06/2022 15:22:30 Processed by : System Administrator
<Chromatogram>
mAU
PDA Multi 1 254nm,4nm
125
Luong dung moi chiet 25ml
15.040
100
75
50
10.191
12.202
25
0
0 5 10 15 20
min
<Peak Table>
PDA Ch1 254nm
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 10.191 | 137158 | 3123 | 2.992 | |||
2 | 12.202 | 33172 | 720 | 0.724 | |||
3 | 15.040 | 4413914 | 123599 | 96.284 | S | ||
Total | 4584244 | 127442 |
D:co thuanoxostephanin22-06-1025 ml.lcd
7/22/2022 3:29:57 PM Page 1 / 1
Analysis Report
<Sample Information>
: 50 ml | |||
Sample ID | : 50 ml | ||
Data Filename | : 50 ml.lcd | ||
Method Filename | : 21-12-01 ÐL oxo trong DL.lcm | ||
Batch Filename | : batch khao sat luong DM.lcb | ||
Vial # | : 1-7 | Sample Type | : Unknown |
Injection Volume | : 20 uL | ||
Date Acquired | : 10/06/2022 15:23:00 | Acquired by | : System Administrator |
Date Processed | : 10/06/2022 17:13:40 | Processed by | : System Administrator |
<Chromatogram>
mAU
PDA Multi 1 254nm,4nm
75
15.094
Luong dung moi chiet 50ml
50
25
10.205
0
0 5 10 15 20
min
<Peak Table>
PDA Ch1 254nm
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 10.205 | 84869 | 1996 | 3.201 | |||
2 | 15.094 | 2566491 | 73151 | 96.799 | M | ||
Total | 2651360 | 75147 |
D:co thuanoxostephanin22-06-1050 ml.lcd
7/22/2022 3:34:54 PM Page 1 / 1
Analysis Report
<Sample Information>
: 100 ml | |||
Sample ID | : 100 ml | ||
Data Filename | : 100 ml.lcd | ||
Method Filename | : 21-12-01 ÐL oxo trong DL.lcm | ||
Batch Filename | : batch khao sat luong DM.lcb | ||
Vial # | : 1-8 | Sample Type | : Unknown |
Injection Volume | : 20 uL | ||
Date Acquired | : 10/06/2022 15:48:33 | Acquired by | : System Administrator |
Date Processed | : 10/06/2022 16:24:16 | Processed by | : System Administrator |
<Chromatogram>
mAU
Luong dung moi chiet 100ml
PDA Multi 1 254nm,4nm
15.139
30
20
10.197
10
0
0 5 10 15 20
min
<Peak Table>
PDA Ch1 254nm
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 10.197 | 31521 | 848 | 0.000 | |||
2 | 15.139 | 1308321 | 37363 | 0.000 | M | ||
Total | 1339842 | 38211 |
D:co thuanoxostephanin22-06-10100 ml.lcd
Phụ lục 4.2.3. Sắc ký đồ các mẫu khảo sát thời gian chiết
7/22/2022 3:43:50 PM Page 1 / 1
Analysis Report
<Sample Information>
: BV1.1.1 | |||
Sample ID | : BV1.1.1 | ||
Data Filename | : BV1.1.1.lcd | ||
Method Filename | : 21-12-01 ÐL oxo trong DL.lcm | ||
Batch Filename | : bacth LOQ.lcb | ||
Vial # | : 1-15 | Sample Type | : Unknown |
Injection Volume | : 20 uL | ||
Date Acquired | : 24/12/2021 21:44:54 | Acquired by | : System Administrator |
Date Processed | : 24/12/2021 22:09:56 | Processed by | : System Administrator |
<Chromatogram>
mAU
PDA Multi 1 254nm,4nm
50
Chiet 3 lan/1 gio
6.840
15.805
40
30
20
5.953
8.618
10.839
13.103
10
0
0 5 10 15 20
min
<Peak Table>
PDA Ch1 254nm
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 5.953 | 131491 | 5736 | 0.000 | |||
2 | 6.840 | 1418867 | 43851 | 0.000 | V | ||
3 | 8.618 | 8090 | 295 | 0.000 | |||
4 | 10.839 | 110404 | 2041 | 0.000 | |||
5 | 13.103 | 43556 | 1138 | 0.000 | |||
6 | 15.805 | 1901511 | 49747 | 0.000 | V | ||
Total | 3613920 | 102809 |
D:co thuanoxostephanin21-12-24BV1.1.1.lcd
7/22/2022 3:45:18 PM Page 1 / 1
Analysis Report
<Sample Information>
: BV1.2.1 | |||
Sample ID | : BV1.2.1 | ||
Data Filename | : BV1.2.1.lcd | ||
Method Filename | : 21-12-01 ÐL oxo trong DL.lcm | ||
Batch Filename | : bacth LOQ.lcb | ||
Vial # | : 1-18 | Sample Type | : Unknown |
Injection Volume | : 20 uL | ||
Date Acquired | : 24/12/2021 23:01:33 | Acquired by | : System Administrator |
Date Processed | : 24/12/2021 23:26:36 | Processed by | : System Administrator |
<Chromatogram>
mAU
Chiet 3 lan/2h
PDA Multi 1 254nm,4nm
6.843
15.824
50
5.962
25
8.554
9.195
10.911
13.121
0
0 5 10 15 20
min
<Peak Table>
PDA Ch1 254nm
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 5.962 | 161631 | 6976 | 0.000 | |||
2 | 6.843 | 1732498 | 54357 | 0.000 | V | ||
3 | 8.554 | 17199 | 486 | 0.000 | |||
4 | 9.195 | 9391 | 282 | 0.000 | V | ||
5 | 10.911 | 225153 | 3065 | 0.000 | |||
6 | 13.121 | 42043 | 1040 | 0.000 | V | ||
7 | 15.824 | 2321195 | 60469 | 0.000 | SV | ||
Total | 4509110 | 126674 |
D:co thuanoxostephanin21-12-24BV1.2.1.lcd
7/22/2022 3:46:07 PM Page 1 / 1
Analysis Report
<Sample Information>
: BV1.3.1 | |||
Sample ID | : BV1.3.1 | ||
Data Filename | : BV1.3.1.lcd | ||
Method Filename | : 21-12-01 ÐL oxo trong DL.lcm | ||
Batch Filename | : bacth LOQ.lcb | ||
Vial # | : 1-21 | Sample Type | : Unknown |
Injection Volume | : 20 uL | ||
Date Acquired | : 25/12/2021 00:43:43 | Acquired by | : System Administrator |
Date Processed | : 25/12/2021 01:08:45 | Processed by | : System Administrator |
<Chromatogram>
6.860
15.851
mAU
Chiet 3 lan/3h
PDA Multi 1 254nm,4nm
50
5.976
25
8.604
10.894
13.205
0
0 5 10 15 20
min
<Peak Table>
PDA Ch1 254nm
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 5.976 | 189101 | 8055 | 0.000 | |||
2 | 6.860 | 1880223 | 59733 | 0.000 | V | ||
3 | 8.604 | 10207 | 384 | 0.000 | |||
4 | 10.894 | 161638 | 2950 | 0.000 | |||
5 | 13.205 | 30418 | 807 | 0.000 | |||
6 | 15.851 | 2550826 | 66340 | 0.000 | SV | ||
Total | 4822412 | 138268 |
D:co thuanoxostephanin21-12-24BV1.3.1.lcd