7/22/2022 3:47:13 PM Page 1 / 1
Analysis Report
<Sample Information>
: BV1.4.1 | |||
Sample ID | : BV1.4.1 | ||
Data Filename | : BV1.4.1.lcd | ||
Method Filename | : 21-12-01 ÐL oxo trong DL.lcm | ||
Batch Filename | : bacth LOQ.lcb | ||
Vial # | : 1-24 | Sample Type | : Unknown |
Injection Volume | : 20 uL | ||
Date Acquired | : 25/12/2021 02:00:22 | Acquired by | : System Administrator |
Date Processed | : 25/12/2021 02:25:24 | Processed by | : System Administrator |
Có thể bạn quan tâm!
-
Hợp Chất Sd11: (6R,9S)-Roseosid -
Sắc Ký Đồ Các Mẫu Khảo Sát Phương Pháp Xử Lý Mẫu -
Sắc Ký Đồ Các Mẫu Khảo Sát Lượng Dung Môi Chiết -
Sắc Ký Đồ Các Mẫu Thẩm Định Độ Lặp Lại -
Sắc Ký Đồ Các Mẫu Thẩm Định Độ Đúng -
Hình Thái Các Dòng Tế Bào Dưới Tác Dụng Của Sd1, Sd2, Sd3, Sd4, Sd5 Tại Thời Điểm 48H (Vk 10X, Zoom 5,6)
Xem toàn bộ 368 trang tài liệu này.
<Chromatogram>
6.859
15.860
mAU
Chiet 3 lan/4h
PDA Multi 1 254nm,4nm
50
5.969
25
8.587
10.943
13.197
0
0 5 10 15 20
min
<Peak Table>
PDA Ch1 254nm
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 5.969 | 197032 | 8234 | 0.000 | |||
2 | 6.859 | 1965026 | 63142 | 0.000 | V | ||
3 | 8.587 | 11349 | 432 | 0.000 | |||
4 | 10.943 | 270507 | 3302 | 0.000 | |||
5 | 13.197 | 39790 | 900 | 0.000 | V | ||
6 | 15.860 | 2689329 | 69846 | 0.000 | SV | ||
Total | 5173034 | 145857 |
D:co thuanoxostephanin21-12-24BV1.4.1.lcd
Phụ lục 4.3. Sắc ký đồ các mẫu thẩm định phương pháp phân tích
Phụ lục 4.3.1. Sắc ký đồ các mẫu thẩm định độ phù hợp hệ thống
5/3/2019 12:34:37 PM Page 1 / 1
Analysis Report
<Sample Information>
Sample Name :
Sample ID :
Data Filename : oxo chuan 25ug 19-3-2019.lcd
Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :
Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL
Date Acquired : 3/19/2019 7:30:36 PM Acquired by : System Administrator Date Processed : 3/19/2019 7:51:39 PM Processed by : System Administrator
<Chromatogram>
14.111
mAU
PDA Multi 1 254nm,4nm
30
20
10
2.589
3.288
0
0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0
min
<Peak Table>
PDA Ch1 254nm
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 2.589 | 18451 | 2032 | 0.000 | |||
2 | 3.288 | 5923 | 131 | 0.000 | |||
3 | 14.111 | 1214153 | 34814 | 0.000 | |||
Total | 1238527 | 36978 |
D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 25ug 19-3-2019.lcd
5/3/2019 12:34:37 PM Page 1 / 1
Analysis Report
<Sample Information>
Sample Name :
Sample ID :
Data Filename : oxo chuan 25ug l2 19-3-2019.lcd
Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :
Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL
Date Acquired : 3/19/2019 9:36:54 PM Acquired by : System Administrator Date Processed : 3/19/2019 9:54:39 PM Processed by : System Administrator
<Chromatogram>
14.148
mAU
PDA Multi 1 254nm,4nm
30
20
2.596
10
3.283
0
0.0 2.5 5.0 7.5 10.0 12.5 15.0
<Peak Table>
PDA Ch1 254nm
min
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 2.596 | 21346 | 2332 | 0.000 | |||
2 | 3.283 | 5851 | 146 | 0.000 | |||
3 | 14.148 | 1219037 | 35210 | 0.000 | |||
Total | 1246234 | 37688 |
D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 25ug l2 19-3-2019.lcd
5/3/2019 12:34:36 PM Page 1 / 1
Analysis Report
<Sample Information>
Sample Name :
Sample ID :
Data Filename : oxo chuan 25ug L3 19-3-2019.lcd
Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :
Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL
Date Acquired : 3/20/2019 3:28:39 PM Acquired by : System Administrator Date Processed : 3/20/2019 3:48:13 PM Processed by : System Administrator
<Chromatogram>
14.334
mAU
PDA Multi 1 254nm,4nm
30
20
10
2.603
3.290
0
0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5
<Peak Table>
PDA Ch1 254nm
min
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 2.603 | 19549 | 2199 | 0.000 | |||
2 | 3.290 | 6062 | 134 | 0.000 | |||
3 | 14.334 | 1215144 | 35147 | 0.000 | |||
Total | 1240755 | 37480 |
D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 25ug L3 19-3-2019.lcd
5/3/2019 12:34:35 PM Page 1 / 1
Analysis Report
<Sample Information>
Sample Name :
Sample ID :
Data Filename : oxo chuan 25ug L4 19-3-2019.lcd
Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :
Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL
Date Acquired : 3/20/2019 3:49:13 PM Acquired by : System Administrator Date Processed : 3/20/2019 4:07:56 PM Processed by : System Administrator
<Chromatogram>
mAU
PDA Multi 1 254nm,4nm
14.320
30
20
2.604
10
0
0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5
<Peak Table>
PDA Ch1 254nm
min
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 2.604 | 23228 | 2472 | 0.000 | V | ||
2 | 14.320 | 1227682 | 34889 | 0.000 | |||
Total | 1250910 | 37362 |
D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 25ug L4 19-3-2019.lcd
5/3/2019 12:34:34 PM Page 1 / 1
Analysis Report
<Sample Information>
Sample Name :
Sample ID :
Data Filename : oxo chuan 25ug L5 19-3-2019.lcd
Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :
Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL
Date Acquired : 3/20/2019 4:09:16 PM Acquired by : System Administrator Date Processed : 3/20/2019 4:28:42 PM Processed by : System Administrator
<Chromatogram>
mAU
PDA Multi 1 254nm,4nm
14.307
30
20
2.601
10
0
0.0 2.5 5.0 7.5 10.0 12.5 15.0 17.5
<Peak Table>
PDA Ch1 254nm
min
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 2.601 | 24672 | 2461 | 0.000 | |||
2 | 14.307 | 1240081 | 35070 | 0.000 | |||
Total | 1264753 | 37530 |
D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 25ug L5 19-3-2019.lcd
5/3/2019 12:34:34 PM Page 1 / 1
Analysis Report
<Sample Information>
Sample Name :
Sample ID :
Data Filename : oxo chuan 25ug L6 19-3-2019.lcd
Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :
Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL
Date Acquired : 3/20/2019 4:29:42 PM Acquired by : System Administrator Date Processed : 3/20/2019 4:47:11 PM Processed by : System Administrator
<Chromatogram>
mAU
PDA Multi 1 254nm,4nm
14.300
30
20
2.596
10
3.287
0
0.0 2.5 5.0 7.5 10.0 12.5 15.0
<Peak Table>
PDA Ch1 254nm
min
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 2.596 | 21153 | 2352 | 0.000 | |||
2 | 3.287 | 6753 | 161 | 0.000 | |||
3 | 14.300 | 1227474 | 34996 | 0.000 | |||
Total | 1255380 | 37509 |
D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 25ug L6 19-3-2019.lcd
Phụ lục 4.3.2. Sắc ký đồ các mẫu thẩm định khoảng tuyến tính và đường chuẩn
3/21/2019 7:04:43 PM Page 1 / 1
Analysis Report
<Sample Information>
Sample Name :
Sample ID :
Data Filename : oxo chuan 3.125ug 19-3-2019.lcd
Method Filename : oxo-MeOH-35-0.1%acid formic-19-3-2019.lcm Batch Filename :
Vial # : 1-1 Sample Type : Unknown Injection Volume : 10 uL
Date Acquired : 3/19/2019 8:37:59 PM Acquired by : System Administrator Date Processed : 3/19/2019 8:54:57 PM Processed by : System Administrator
<Chromatogram>
mAU
PDA Multi 1 254nm,4nm
14.185
7.5
5.0
2.597
2.5
2.443
0.0
0.0 2.5 5.0 7.5 10.0 12.5 15.0
<Peak Table>
PDA Ch1 254nm
min
Ret. Time | Area | Height | Conc. | Unit | Mark | Name | |
1 | 2.443 | 1282 | 147 | 0.000 | |||
2 | 2.597 | 22209 | 2449 | 0.000 | V | ||
3 | 14.185 | 272443 | 7965 | 0.000 | |||
Total | 295934 | 10560 |
D:HLSONthao-diemoxo chuan 19-3-2019oxo chuan 3.125ug 19-3-2019.lcd