APPENDIX 4.6
NMR AND MS SPECTRUM DATA OF COMPOUND PT6
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1 H-NMR spectrum of compound PT6 (20.3 mg) measured in CD 3 OD
13 C-NMR spectrum of compound PT6 (20.3 mg) measured in CD 3 OD
DEPT-NMR spectrum of compound PT6 (20.3 mg) measured in CD 3 OD
- Scan (0.10640000000000000000-0.19818333333333300000 min, 23 Scans) C2.d
321.0597
170.8343
194.0215
134.8662
303.0494
352.0735
i,
1.
x10 5
1.05—
1
0.95
0.9
0.85
0.8
0.75
0.7
0.65
0.6
0.55
0.5
0.45
0.4
0.35
0.3
0.25
0.2
0.15
0.1
0.05
0—
130 140 150 160 170 180 190 200 210 220 230 240 250 260 270 280 290 300 310 320 330 340 350 360
Counts vs. Mass-to-Charge (m/z)
HR-ESI-MS [M+H] + spectrum of compound PT6 (20.3 mg)